Some critical aspects of FT-IR, TGA, powder XRD, EDAX and SEM studies of calcium oxalate urinary calculi.

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dc.contributor.authorJoshi, Vimal S
dc.contributor.authorVasant, Sonal R
dc.contributor.authorBhatt, J G
dc.contributor.authorJoshi, Mihir J
dc.date.accessioned2014-12-26T09:54:28Z
dc.date.available2014-12-26T09:54:28Z
dc.date.issued2014-06
dc.description.abstractUrinary calculi constitute one of the oldest afflictions of humans as well as animals, which are occurring globally. The calculi vary in shape, size and composition, which influence their clinical course. They are usually of the mixed-type with varying percentages of the ingredients. In medical management of urinary calculi, either the nature of calculi is to be known or the exact composition of calculi is required. In the present study, two selected calculi were recovered after surgery from two different patients for detailed examination and investigated by using Fourier-Transform infrared spectroscopy (FT-IR), thermo-gravimetric analysis (TGA), powder X-ray diffraction (XRD), scanning electron microscopy and energy dispersive analysis of X-rays (EDAX) techniques. The study demonstrated that the nature of urinary calculi and presence of major phase in mixed calculi could be identified by FT-IR, TGA and powder XRD, however, the exact content of various elements could be found by EDAX only.en_US
dc.identifier.citationJoshi Vimal S, Vasant Sonal R, Bhatt J G, Joshi Mihir J. Some critical aspects of FT-IR, TGA, powder XRD, EDAX and SEM studies of calcium oxalate urinary calculi. Indian Journal of Biochemistry & Biophysics. 2014 Jun; 51(3): 237-243.en_US
dc.identifier.urihttps://imsear.searo.who.int/handle/123456789/154236
dc.language.isoenen_US
dc.source.urihttps://nopr.niscair.res.in/handle/123456789/29090en_US
dc.subjectUrinary calculien_US
dc.subjectCharacterizationen_US
dc.subjectCalcium oxalate monohydrateen_US
dc.subjectPhosphate impuritiesen_US
dc.subject.meshAged
dc.subject.meshCalcium Oxalate --chemistry
dc.subject.meshFemale
dc.subject.meshHumans
dc.subject.meshMale
dc.subject.meshMicroscopy, Electron, Scanning --methods
dc.subject.meshMiddle Aged
dc.subject.meshPowders
dc.subject.meshSpectroscopy, X-Ray Emission --methods
dc.subject.meshSpectroscopy, Fourier Transform Infrared --methods
dc.subject.meshThermogravimetry --methods
dc.subject.meshUrinary Calculi --chemistry
dc.subject.meshX-Ray Diffraction --methods
dc.titleSome critical aspects of FT-IR, TGA, powder XRD, EDAX and SEM studies of calcium oxalate urinary calculi.en_US
dc.typeArticleen_US
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